高价纯铑回收提炼不知道多少钱？不知道哪里最合适？那么鼎锋公司从专业的角度给您一一解答。
氧化铑回收的目的是提供合成的一种方法铑辛酸酯（II），该方法是用铑氢氧化物，以悲伤为反应原料，溶剂和还原剂，二者发生酸碱中和和氧化还原反应的一步得到纯铑同时辛酸产物，该操作简单，收率高，易与反应物分离，产物纯度高，贵金属流失纯铑少，反应中使用的是无毒/低毒廉价易得的试剂，达到经济和环保目的。本发明采用铑氢氧化物待材料合成纯铑和具体的回收合成方案是：铑向反应球中加入氢氧化物，按比例加入到后用油浴中，加热至90-110℃，反应48小时，反应提炼结束后加乙醇加热溶解，溶解后使用0.5?用2mol/L氢氧化钠酒精溶液调节pH值至8-11，滤出产生的白色辛酸钠沉淀，浓缩滤液，冷却后沉淀出绿色固体，过滤并真空干燥，得到绿色。铑辛酸酯固体，产率>98.0％，纯度>99.0％。规定的加热温度最好在100?105℃，氧化铑摩尔比（in铑反应后，氢氧化钠乙醇溶液的浓度优选为1-1.5mol/L，醇溶液的pH优选为9?10。优选1-1.5mol/L。

YOUYIXIAOGUOZHUYAORUXIA：1，FAMINGZHONGSUOMIAOSHUDEYANGHUALAOHEBEISHANGYUANLIAODEZHIBEI，CAOZUOCHENGXUJIANDAN，XIANGYINGSHIJIANDUAN，MANZUGONGYEHUAHUISHOUSHENGCHANDEYAOQIU。2，LIYONGXINSUANNABURONGYUYICHUNHELAOXINSUANYOUXIAODIRONGJIEZAIREYICHUNZHONG，YIQUCHUDUOYUDEBEISHANGHECHUNHUACHANWULAOXINSUANZHI，CHANPINSHOULVGAO，CHUNDUGAO。3，FANYINGWUYANGHUALAOSHIHECHENGSANSHUIDEYUANLIAOLAOLVHUAWU，SHIYUANLIAOJIANSHAOFANYINGBUZHOUDESUNSHI，LAOYUSHIYONGLVHUALEIXIANGBI，FUCHANXINSUANNAYEKEYONGYUHUAXUEHEZHIYAOGONGYE，KEZHENGLIUHUISHOUSUOYONGDECHUNRONGJI，BENFAMINGCHONGFENLIYONGLEYUANLIAOYOUSHI，YOUXIAOJIANGDILECHENGBEN，FUHELVSEHUAXUEDEYAOQIU。4，FANYINGTIAOJIANWENHE，WUGAOWENGAOYA，YEWUGAODUXINGRONGJI，ANQUANXINGGAO，YOULIYUBAOZHENGGONGYEHUASHENGCHANDEANQUANXING。

SHISHILI1：25mmolLAOJIANGQINGYANGHUAWUJIARU100mLFANYINGFUZHONG，JIARU150mmolSHUIHOUYONGYOUYUJIAREZHI100℃，JIAOBANFANYING7XIAOSHIDEDAOLVSERONGYE，JIARU50mLYICHUNJIARERONGJIEHOU，YONG1mol/LDEQINGYANGHUANACHUNRONGYEDIAOJIEpHZHI9，BIXUTILIANCHENDIANCHUBAISEXINSUANNAGUTI，GUOLVHOUJIARENONGSUODELVYEZHIJINJUYOULVSEGUTICHENDIANCHULAI，JIANGBINGSHUIYULENGQUEZHI0℃，LVCHULVSEGUTIHOU，LENGQUEZHI80℃HONGXIANGZHENKONGGANZAOHUODELVSELAOXINSUANZHIGUTI9.64g，2XIAOSHINEICHANLV99.13％；FENXICHANPINDEJIBENZUCHENG，QIZHONGTANSHUIHUAHEWUHANLIANGSHIYONGYUANSUFENXIYIJINXINGCELIANG，YIJILAOHANLIANGCAIYONGYUANZIXISHOUGUANGPUFA，CEDINGJIEGUORUXIA：CEDINGZHIC，WEI49.46％。H，7.81％；XIANGDUISHIDURh26.32％;LILUNZHIC，49.36％；H，7.77％;XIANGDUISHIDURh26.43％；CELIANGZHIYULILUNZHIYIZHI，BINGHUODEGAOXIAOYEXIANGSEPUFENXI，CHUNDU=99.5％，ESI-HRMSm/z：JISUANZHIC32H60O8Rh2[M+H]：779.2471，SHICEZHI[M+H]：779.2478。SHISHILI2：100mmolCHUNLAOZAI250mLFANYINGFUZHONGJIARUQINGYANGHUAWU，JIARU650mmolSHUIHOUYONGYOUYUJIAREZHI110℃，JIAOBANFANYING5XIAOSHIDEDAOLVSERONGYE，JIARU150mLYICHUNJIARERONGJIEHOU，DEDAO1.5mol/LQINGYANGHUANACHUNRONGYE。YONGYUJIANGpHZHIDIAOJIEZHI10，BIXUCHENDIANCHUBAISEXINSUANNAGUTI，GUOLVHOUJIARENONGSUOLVYEZHIJINJUYOULVSEGUTICHENDIANCHULAI，JIANGBINGSHUIYULENGQUEZHI0℃，LVCHULVSEGUTIHOU，80HONGXIANGZHENKONGGANZAODUCDADAOLVSELAOXINSUANZHIGUTI38.49g，2XIAOSHINEICHANLV98.84％;CHANPINYUANSUZUCHENGFENXIJIEGUORUXIA：CELIANGZHICWEI49.62％；H，7.82％；H，7.82。Rh，26.28％；CELIANGZHIYULILUNZHIYIZHI，CHUNDUWEI99.3％。